Agitator Tip Velocity
agitator tip velocity is an important factor to consider. It refers to the speed at which the agitator blades move through the liquid in the reactor. This velocity can affect the mixing efficiency and the heat transfer rate in the reactor.
Tip velocity of agitator means rotation speed of agiatator. It is expressed as m/sec. Mixing intensity depends on rotation of agitator.
It means mixing intensity of different agitator is same if tip velocity is same, Answer is no.
Tip Velocity (V) = π x D x N
Where,
V = Velocity in m/s
D = Diameter of agitator in m
N= Rotation per second
Example :
Reactor with capacity 5 KL agitator running with 75 rpm. Agitator diameter is 1200 mm.
Calculate : Tip velocity in m/sec.
Sol:
Given : rpm = 75, rps = 1.25
Agitator Dia. = 1200 mm = 1.2 m
Tip velocity = π.D.N = 3.14 x 1.2 x 1.25 ( m/sec)
= 4.71 m/sec
Agitator power calculation
Agitatator power calculation important for ensuring suitability of use as well as mapping equipment during technolgy transfer for same volume or increased volume.
Pharmaceutical applications :
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Agitator power should be same for identical reactor and same volume of handling.
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Reaction volume required power should be maximum 75 % of rated capacity provided by reactor designer.
Formula :
P = n x Np x ρ x N^3 x D^5
Where,
P = Agitator Power watt ( W)
1 KW = 1000 W
1 HP = 746 W
n = No. agitator stages
Np = Power No.
N = Rotation per sec
D = Dia. Of Agitator in m
ρ = Density in kg/m3
Example :
Reactor Anchor running with 75 rpm. Agitator diameter is 1200 mm, liquid viscosity is 1.2 kg/m.sec and density 1000 kg/m3.
Calculate : Agitator Power
Sol:
Given : rpm = 75/60 = 1.25 RPS, n = 1,
Np = 0.6, Density = 1000 kg/m3, Dia. = 1200 = 1.2 m
Agitator Power = n x Np x ρ x N^3 x D^5 =1 x 0.6 x 1000 x 1.25^3 x 1.2^5 = 2916 W= 2.91 KW= 3.9 HP
Considering Motor efficiency & transmission losses, Agitator Power = 3.9 / 0.8 = 4.87 i.e. 5 HP
Tip Velocity : Vt ( m/sec )
= π Da N
N = rotational speed in seconds
Da = agitator swip dia. m
Example
Reactor with capacity 5 KL agitator running with 75 rpm agitator diameter is 1200mm
Calculate Tip velocity
Solution. :
Given
Da = 1200 mm = 1.2 m
N = 75 rpm = 1.25 rps
Vt =π Da N
Vt = 3.142 X 1.2 X 1.25 = 4.71 m/s
Reynold's Number : NRE
= (ρ∗N∗Da2 )/µ
Where,
ρ = density of liquid kg/m3
N = rotational speed in seconds
Da = agitator swip dia. m
µ = viscosity of liquid kg/m sec
Example
Reactor agitator running with 75 rpm. Agitator diameter is 1200 mm,
Liquid viscosity is 1200 cp and density is 1800 kg/m3
calculate
Reynolds number NRE
solution :
Given viscosity = 1200 cp = 1.2 kg/m.s
RPM= 75 = 1.25 rps
Density = 1800 kg / m3
NRE = (ρ∗N∗Da2 ) = 2700
Agitator Power Watt : P
= Np ρ * N3 * Da5
ρ= density of liquid kg/m3
N = rotational speed in seconds
Da = agitator swip dia. m
Np= power number
Example
Reactor running with 75 rpm . Agitator diameter is 1200mm, Liquid viscosity is 1.2 kg/m.s and density 1000 kg/m3 .
Calculate Agitator power
Solution :
Given ρ = 1000 kg/m3 N= 1.25 rps Da = 1.2 m Np = 0.6
Agitator power = Np* ρ *N^3* Da^5
= 0.6 x 1000 x 1.25^3 * 1.25 ^5
= 2916 W = 2.916 KW = 3.9 HP
Power / Volume (W/lt)
= (Np ∗ρ ∗ N3 ∗Da5 )/Vmass
ρ = density of liquid kg/m3
N = rotational speed in seconds
Da = agitator swip dia. m
Np= power number
Vmass = Liquid volume in lt.
Example
Reactor running with 75 rpm . Agitator diameter is 1200mm, Liquid viscosity is 1.2 kg/m.s and density 1000 kg/m3 .
Reaction mass volume 1500 lt.
Calculate : Agitator power / volume
Solution :
Given
ρ = 1000 kg/m3 N= 1.25 rps Da = 1.2 m , Np = 0.6 V = 1500 lt
Agitator power = (Np ∗ ρ ∗ N3 ∗ Da5)/(Vmass )
= (0.6 ∗ 1000∗ 1.25^3 ∗ 1.25^5 )/1500
= 1.944 W/ lt
Agitator Pumping Capacity : Q in m3/s
= NQ N Da3
N = rotational speed in seconds
Da = agitator swip dia. in m
NQ = flow number
Example
Reactor running with 75 rpm . Agitator diameter is 600mm, reactor diameter is 1100 mm and density 1000 kg/m3
Calculate Agitator pumping capacity
Solution :
Given
NQ = 0.6
N = 75 rpm = 1.25 rps ,
Da = 0.6 m
Q = NQ N Da3
= 0.6 X 1.25 X 0.6^3 = 0.16 m3/s
Mixing time : tm in sec
= 5∗ Vmass)/NQ ∗ N ∗ Da^3
N = rotational speed in seconds
Da = agitator swip dia. m
NQ = flow number `
Vmass = Liquid volume m3
Example
Reactor with capacity 5 KL contain 1.5 KL of liquid , running with 90 rpm. Agitator diameter is 1200 mm
Calculate : Mixing time
Solution :
Given
V mass = 1.5 m3
NQ= 0.5 ( for anchor ) ,
N = 90 rpm ( 1.5 rps ),
Da = 1200 mm = 1.2 m
tm = 5∗ Vmass)/NQ ∗ N ∗ Da^3 =5 x 1.5 / 0.6∗ 1.5 ∗ 1.2^3 = 4.82 s
Shear rate
= [P/(v∗ µ)) ] ^0.5
r = average shear rate (S-1 )
P = Agitator power in W
µ = Liquid viscosity (Pa . S) or kg/m s or poise
1 Pa. s = 10 Poise
V = liquid volume in m3
Example
A Reactor contain 2000 L of Liquid , Agitator power is 2916 W, viscosity of liquid is 1.2 pa. s
Calculate shear rate
Solution :
Given
V = 2 m3 P = 2916 W µ = 1.2 pa.s
r = [P/(V ∗ µ)) ] ^ 0.5 = [2916/(2∗1.2 )) ] ^0.5 = 34.85 S-1
Just Suspension speed (NJS) (Sec)
= S v^0.1 [g (ρS – ρL)/ρL ]0.45 X^0.13 dp^0.2 D^–0.85
NJS= just suspension speed, rps
S= geometry factor
dp= Particle diameter, m
g = gravitational acceleration, m/s2
ρL = Liquid density , kg/m3
ρs = Solid density, kg/m3
D = impeller diameter, m
X= Wt. of solid / wt. of liquid x 100, %
v= Kinematic viscosity, m2/s
v = µ / ρ
µ = Dynamic viscosity in kg/m.s or pa.s or Poise
1 kg/ms or pa. s = 10 poise
Example
Calculate the just suspension impeller speed for AICI. The impeller is 45° a pitched blade with D/T value of 1/3 ànd blade width of D/4 located.
Calculate : NJS in rps
Solution :
Given
S= 3.7
dp= 5000 µm ( 0.005 m )
g = 9.81 m/s2
ρL = 1326 kg/m3
ρs = 2440 kg/m3
D = 0.724 m
X= 0.4
µ = 1 cp = 0.001 kg /s
v = µ / ρ
v = 7.54 * 10-7 m2/s
Njs = = S v^0.1 [g (ρS – ρL)/ρL ]0.45 X^0.13 dp^0.2 D^–0.85
= 3.7* (7.54 10^-7)^0.1 [9.81 x (2440 – 1326) /326 ]^0.45 0.4^ 0.13 0.005 ^0.2 0.724^–0.85
= 0.95 rps =57 rpm
Batch reactor heat transfer area :
Cylindrical section + Torispherical section
πDL + [ (ᴫ/24 )∗ ((1.147 ∗ D)^2) ]
Where,
D=Diameter of reactor cylindrical section in m
L =Height of cylindrical section in m
Reactor condenser sizing m2
Ac = (UR ∗AR ∗LMTD rea )/(Uc ∗LMTD cond)
UR = reactor jacket overall HTC, kcal/hr.m2. °C
AR = Jacket heating area, m2
Uc = Condenser overall HTC, kcal/hr.m2. °C
Example
A stainless steel reactor having capacity 4 KL. Reactor subjected to maximum temperature 25 °C
( LMTD = 20 °C ) jacket side . Condenser side ( LMTD = 25 °C ).
Calculate reactor condenser sizing in m2
Solution :
Given
V = 4 KL
UR = 300 kcal/hr m2 °C
Uc = 350 kcal / hr.m2. °C
LMTD rea = 20 °C
LMTD cond = 25 °C
Reactor surface area = 3.8 V0.68 = 3.8 40.68 = 9.75 m2
Ac = (UR ∗AR ∗LMTD rea )/(Uc ∗LMTD cond) =(300∗9.75∗20)/(350∗25)) = 6.68 m2
Reactor vent sizing mm2
= 179400 ∗Q∗√(T∗G∗Z))/(C ∗ K ∗ P1 ∗ kb ))
Q=Required relieving capacity, m3/min
C = coeffient For sp. Heats ( use value 315 )
T= temp in ℃
G=sp. Gravity of gas
Z=Compressibility factor ( used value 1 )
K=coefficient of discharge ( used value 0.975 )
P1=Relieving pressure, abs+guage+21% excess in kPa
Kb= capacity correction factor ( use value 1 )
Example
Rate of vaporization of ethylene gas vapour through the reactor vent at flow rate Q is 326 m3/min T is 93 ℃ and P is 1170 Kpa. Calculate reactor vent size
Given
Q= 326 m3 / min
P 405.3 Kpa
T =93 ℃ =366 k
G= 0.78
Z= 1
K = 0.975
P1 = 1170 + 245.7 + 110 = 1525.7 kpa
Kb = 1
C = 315
Solution :
Reactor vent size
= 79400 ∗Q∗√(T∗G∗Z))/(C ∗ K ∗ P1 ∗ kb ))
= (179400 ∗326∗ 36√(366∗0.78∗1))/(1∗ 315 ∗0.975 ∗1525.7 ))
= 2346 mm2
Liquid effective agitation depth : dp in m
= =(Rvol -Rt )/(ᴫ/4∗DR^2))
(Rvol = reaction mass volume m3
DR = reactor internal dia. m
Rt = Torispherical volume = (ᴫ/24 ∗DR3)
Example
A stainless steel reactor having diameter 1800 mm contain reaction mass volume 1 KL
Calculate liquid effective agitation depth
Solution :
Given
DR= 1800 mm = 1.8 m
Rvol = 1 KL = 1 m3
Rt = ᴫ/24 ∗DR3 = 0.7635 m2
dp = (Rvol -Rt )/(ᴫ/4 ∗DR^2) = (1-0.7635)/2.54) = 0.092 m